Simultaneous thermal analysis (setline STA)
Simple & Powerful
Simultaneous thermal analysis (STA) is the combination of thermogravimetric analysis (TGA) and differential thermal analysis (DTA) or differential scanning calorimetry (DSC). The mass change and heat flow change can be obtained once measurement on one instrument.
APPLICATIONS
Adsorption | Catalytic reaction | Compositional analysis |
Corrosion/Oxidation | Crystallization | Curing |
Decomposition | Differential scanning calorimetry | Evaporation |
Glass transition temperature | Magnetic transitions | Mass change |
Phase diagram | Phase transition temperature | Purity determination |
Reaction kinetics | Residual mass | Simultaneous thermal analysis |
Solid-gas reactions | Solid-liquid reactions | Solid-solid reaction |
Specific heat determination | Sublimation | Synthesis reactions |
Thermal stability | Thermogravimetric analysis | Transition enthalpies |
PARAMETERS
Temperature range | RT~1100°C |
Programmable heating rate | 0.01~50°C/min |
Temperature precision | ±0.05°C |
Mass variation resolution | 0.02ug |
Mass variation range | ±1000mg |
Autosampler | 51(sample and reference ) |
For more information, please click on the website(http://www.setaram.cn )
APPLICATIONS
Calcium oxalate monohydrate (CaC2O4,H2O) samples were measured by mass loss (TG) and heat flow (DSC). From lower temperature to higher temperature: dehydration, formation of calcium carbonate and formation of calcium oxide. This simple case highlights the application of thermogravimetric analysis in quantitative measurement.
Analysis of synthetic rubber components.
The sample was heated to 600°C in two steps under an inert atmosphere (N2) and then cooled to 400°C, and the atmosphere was switched to air, the sample was heated to 800°C after holding for a period of time. The TG curve has three mass losses corresponding to the decomposition of plasticizers: oil and wax content (3.6%), elastomer content (57.9%) and carbon black content (38.7%). The remaining mass at the end of the experiment corresponds to the ash content of the rubber (<0.5%).
ASTM Number | Title | Website Link |
E968-02 | Standard Practice for Heat Flow Calibration of Differential Scanning Calorimeters | Link |
E2253-11 | Standard Test Method for Temperature and Enthalpy Measurement Validation of Differential Scanning Calorimeters | Link |
E967-08 | Standard Test Method for Temperature Calibration of Differential Scanning Calorimeters and Differential Thermal Analyzers | Link |
E1356-08 | Standard Test Method for Assignment of the Glass Transition Temperatures by Differential Scanning Calorimetry | Link |
D6604-00 | Standard Practice for Glass Transition Temperatures of Hydrocarbon Resins by Differential Scanning Calorimetry | Link |
E928-08 | Standard Test Method for Purity by Differential Scanning Calorimetry | Link |
E1269-11 | Standard Test Method for Determining Specific Heat Capacity by Differential Scanning Calorimetry | Link |
E537-12 | Standard Test Method for The Thermal Stability of Chemicals by Differential Scanning Calorimetry | Link |
E793-06 | Standard Test Method for Enthalpies of Fusion and Crystallization by Differential Scanning Calorimetry | Link |
D3418-15 | Standard Test Method for Transition Temperatures and Enthalpies of Fusion and Crystallization of Polymers by Differential Scanning Calorimetry | Link |
E2160-04 | Standard Test Method for Heat of Reaction of Thermally Reactive Materials by Differential Scanning Calorimetry | Link |
D4591-07 | Standard Test Method for Determining Temperatures and Heats of Transitions of Fluoropolymers by Differential Scanning Calorimetry | Link |
D3895-14 | Standard Test Method for Oxidative-Induction Time of Polyolefins by Differential Scanning Calorimetry | Link |
E1582-14 | Standard Practice for Calibration of Temperature Scale for Thermogravimetry | Link |
E2040-08 | Standard Test Method for Mass Scale Calibration of Thermogravimetric Analyzers | Link |
E2402-11 | Standard Test Method for Mass Loss and Residue Measurement Validation of Thermogravimetric Analyzers | Link |
E794-06 | Standard Test Method for Melting and Crystallization Temperatures by Thermal Analysis | Link |
E1131-08 | Standard Test Method for Compositional Analysis by Thermogravimetry | Link |
D6370-99 | Standard Test Method for Rubber–Compositional Analysis by Thermogravimetry (TGA) | Link |
E1868-10 | Standard Test Methods for Loss-On-Drying by Thermogravimetry | Link |
E2008-08e1 | Standard Test Methods for Volatility Rate by Thermogravimetry | Link |
E2550-11 | Standard Test Method for Thermal Stability by Thermogravimetry | Link |
D6382-99 | Standard Practice for Dynamic Mechanical Analysis and Thermogravimetry of Roofing and Waterproofing Membrane Material | Link |
E1877-15 | Standard Practice for Calculating Thermal Endurance of Materials from Thermogravimetric Decomposition Data | Link |
E2403-06 | Standard Test Method for Sulfated Ash of Organic Materials by Thermogravimetry | Link |
E2043-99 | Standard Test Method for Nonvolatile Matter of Agricultural Adjuvant Solutions by Thermogravimetry | Link |
D3850-12 | Standard Test Method for Rapid Thermal Degradation of Solid Electrical Insulation Materials By Thermogravimetric Method (TGA) | Link |
ISO Number | Title | Website Link |
11358 | Plastics– Thermogravimetry (TG) of polymers | Link |
9924 | Rubber and rubber products– Determination of the composition of vulcanizates and uncured compounds by thermogravimetry | Link |
21870 | Rubber compounding ingredients– Carbon black– Determination of high-temperature loss on heating by thermogravimetry | Link |
11308 | Nanotechnologies– Characterization of single-wall carbon nanotubes using thermogravimetric analysis | Link |
11357 | Plastics– Differential scanning calorimetry (DSC) | Link |
18373 | Rigid PVC pipes– Differential scanning calorimetry (DSC) method | Link |
15309 | Implants for surgery– Differential scanning calorimetry of poly ether ether ketone (PEEK) polymers and compounds for use in implantable medical devices | Link |
16805 | Binders for paints and varnishes– Determination of glass transition temperature | Link |
28343 | Rubber compounding ingredients– Process oils– Determination of glass transition temperature by DSC | Link |
11409 | Plastics– Phenolic resins– Determination of heats and temperatures of reaction by differential scanning calorimetry | Link |
22768 | Rubber, raw– Determination of the glass transition temperature by differential scanning calorimetry (DSC) | Link |
14322 | Plastics– Epoxy resins– Determination of degree of crosslinking of crosslinked epoxy resinsby differential scanning calorimetry | Link |